A remarkable side-product from the synthesis of an octaalkylphthalocyanine: formation of a tetrabenzotriazaporphyrin

Andrew N. Cammidge; Michael J. Cook; David L. Hughes; Fabien Nekelson; Muhibur Rahman

doi:10.1039/b414820g

A remarkable side-product from the synthesis of an octaalkylphthalocyanine: formation of a tetrabenzotriazaporphyrin

Andrew N. Cammidge
, Michael J. Cook
, David L. Hughes
, Fabien Nekelson
, Muhibur Rahman

Synthetic and Medicinal Chemistry

Research output: Contribution to journal › Article › peer-review

25 Citations (Scopus)

Abstract

1,4,8,11,15,18,22,25-Octahexyl-29H,31H-tetrabenzo[b,g,l,q][5,10,15]triazaporphyrin has been isolated as the main side product in the preparation of 1,4,8,11,15,18,22,25-octahexylphthalocyanine via a lithium pentyloxide induced cyclotetramerisation of 3,6-dihexylphthalonitrile.

Original language	English
Pages (from-to)	930-932
Number of pages	3
Journal	Chemical Communications
Issue number	7
DOIs	https://doi.org/10.1039/b414820g
Publication status	Published - 2005

Access to Document

10.1039/b414820g

Cite this

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title = "A remarkable side-product from the synthesis of an octaalkylphthalocyanine: formation of a tetrabenzotriazaporphyrin",

abstract = "1,4,8,11,15,18,22,25-Octahexyl-29H,31H-tetrabenzo[b,g,l,q][5,10,15]triazaporphyrin has been isolated as the main side product in the preparation of 1,4,8,11,15,18,22,25-octahexylphthalocyanine via a lithium pentyloxide induced cyclotetramerisation of 3,6-dihexylphthalonitrile.",

author = "Cammidge, \{Andrew N.\} and Cook, \{Michael J.\} and Hughes, \{David L.\} and Fabien Nekelson and Muhibur Rahman",

year = "2005",

doi = "10.1039/b414820g",

language = "English",

pages = "930--932",

journal = "Chemical Communications",

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publisher = "Royal Society of Chemistry",

number = "7",

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T1 - A remarkable side-product from the synthesis of an octaalkylphthalocyanine: formation of a tetrabenzotriazaporphyrin

AU - Cammidge, Andrew N.

AU - Cook, Michael J.

AU - Hughes, David L.

AU - Nekelson, Fabien

AU - Rahman, Muhibur

PY - 2005

Y1 - 2005

N2 - 1,4,8,11,15,18,22,25-Octahexyl-29H,31H-tetrabenzo[b,g,l,q][5,10,15]triazaporphyrin has been isolated as the main side product in the preparation of 1,4,8,11,15,18,22,25-octahexylphthalocyanine via a lithium pentyloxide induced cyclotetramerisation of 3,6-dihexylphthalonitrile.

AB - 1,4,8,11,15,18,22,25-Octahexyl-29H,31H-tetrabenzo[b,g,l,q][5,10,15]triazaporphyrin has been isolated as the main side product in the preparation of 1,4,8,11,15,18,22,25-octahexylphthalocyanine via a lithium pentyloxide induced cyclotetramerisation of 3,6-dihexylphthalonitrile.

U2 - 10.1039/b414820g

DO - 10.1039/b414820g

M3 - Article

SN - 1359-7345

SP - 930

EP - 932

JO - Chemical Communications

JF - Chemical Communications

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ER -