Solid state NMR and X-ray diffraction studies of α-d-galacturonic acid monohydrate

Hui-Ru Tang; Peter S. Belton; Sian C. Davies; David L. Hughes

doi:10.1016/S0008-6215(00)00307-4

Solid state NMR and X-ray diffraction studies of α-d-galacturonic acid monohydrate

Hui-Ru Tang, Peter S. Belton, Sian C. Davies, David L. Hughes

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Abstract

Crystalline a-d-galacturonic acid monohydrate has been studied by 13C CPMAS NMR and X-ray crystallography. The molecular dynamics were investigated by evaluating 13C spin-lattice relaxation in the rotating frame (T1?) and chemical-shift-anisotropy properties of each carbon. Only limited molecular motions can be detected in the low frequency (

Original language	English
Pages (from-to)	391-399
Number of pages	9
Journal	Carbohydrate Research
Volume	330
Issue number	3
DOIs	https://doi.org/10.1016/S0008-6215(00)00307-4
Publication status	Published - 2001

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10.1016/S0008-6215(00)00307-4

Cite this

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title = "Solid state NMR and X-ray diffraction studies of α-d-galacturonic acid monohydrate",

abstract = "Crystalline a-d-galacturonic acid monohydrate has been studied by 13C CPMAS NMR and X-ray crystallography. The molecular dynamics were investigated by evaluating 13C spin-lattice relaxation in the rotating frame (T1?) and chemical-shift-anisotropy properties of each carbon. Only limited molecular motions can be detected in the low frequency (",

author = "Hui-Ru Tang and Belton, {Peter S.} and Davies, {Sian C.} and Hughes, {David L.}",

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AU - Belton, Peter S.

AU - Davies, Sian C.

AU - Hughes, David L.

PY - 2001

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AB - Crystalline a-d-galacturonic acid monohydrate has been studied by 13C CPMAS NMR and X-ray crystallography. The molecular dynamics were investigated by evaluating 13C spin-lattice relaxation in the rotating frame (T1?) and chemical-shift-anisotropy properties of each carbon. Only limited molecular motions can be detected in the low frequency (

U2 - 10.1016/S0008-6215(00)00307-4

DO - 10.1016/S0008-6215(00)00307-4

M3 - Article

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VL - 330

SP - 391

EP - 399

JO - Carbohydrate Research

JF - Carbohydrate Research

IS - 3

ER -