Solid state NMR and X-ray diffraction studies of α-d-galacturonic acid monohydrate

Hui-Ru Tang, Peter Belton, Sian C Davies, David Hughes

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Abstract

Crystalline a-d-galacturonic acid monohydrate has been studied by 13C CPMAS NMR and X-ray crystallography. The molecular dynamics were investigated by evaluating 13C spin-lattice relaxation in the rotating frame (T1?) and chemical-shift-anisotropy properties of each carbon. Only limited molecular motions can be detected in the low frequency (
Original languageEnglish
Pages (from-to)391-399
Number of pages9
JournalCarbohydrate Research
Volume330
Issue number3
DOIs
Publication statusPublished - 2001

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