Synthesis of 13C-labelled methyl α - D -mannopyranosyl-(1→2)-α-D-mannopyranoside from [U-13C]-D-glucose

A. K. Misra; J. M. Brown; S. W. Homans; R. A. Field

Synthesis of ¹³C-labelled methyl α - D -mannopyranosyl-(1→2)-α-D-mannopyranoside from [U-¹³C]-D-glucose

A. K. Misra
, J. M. Brown
, S. W. Homans
, R. A. Field

School of Chemistry, Pharmacy and Pharmacology

Research output: Contribution to journal › Article › peer-review

3 Citations (Scopus)

Abstract

The structural basis of lectin-carbohydrate interactions has been an area of interest for many years. With a view to implementing new NMR approaches for studying such interactions we now report the synthesis of methyl 2-O-α-D-mannopyranosyl-α-D-mannopyranoside, a ligand for concanavalin A, from uniformly ¹³C-labelled D-glucose.

Original language	English
Pages (from-to)	217-222
Number of pages	6
Journal	Carbohydrate Letters
Volume	3
Issue number	3
Publication status	Published - 1998

Keywords

C-enrichment
Concanavalin A
Man-α-1,2-Man-α-OMe
NMR spectroscopy

Cite this

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title = "Synthesis of 13C-labelled methyl α - D -mannopyranosyl-(1→2)-α-D-mannopyranoside from [U-13C]-D-glucose",

abstract = "The structural basis of lectin-carbohydrate interactions has been an area of interest for many years. With a view to implementing new NMR approaches for studying such interactions we now report the synthesis of methyl 2-O-α-D-mannopyranosyl-α-D-mannopyranoside, a ligand for concanavalin A, from uniformly 13C-labelled D-glucose.",

keywords = "C-enrichment, Concanavalin A, Man-α-1,2-Man-α-OMe, NMR spectroscopy",

author = "Misra, \{A. K.\} and Brown, \{J. M.\} and Homans, \{S. W.\} and Field, \{R. A.\}",

year = "1998",

language = "English",

volume = "3",

pages = "217--222",

journal = "Carbohydrate Letters",

issn = "1073-5070",

publisher = "Harwood Academic Publishers",

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T1 - Synthesis of 13C-labelled methyl α - D -mannopyranosyl-(1→2)-α-D-mannopyranoside from [U-13C]-D-glucose

AU - Misra, A. K.

AU - Brown, J. M.

AU - Homans, S. W.

AU - Field, R. A.

PY - 1998

Y1 - 1998

N2 - The structural basis of lectin-carbohydrate interactions has been an area of interest for many years. With a view to implementing new NMR approaches for studying such interactions we now report the synthesis of methyl 2-O-α-D-mannopyranosyl-α-D-mannopyranoside, a ligand for concanavalin A, from uniformly 13C-labelled D-glucose.

AB - The structural basis of lectin-carbohydrate interactions has been an area of interest for many years. With a view to implementing new NMR approaches for studying such interactions we now report the synthesis of methyl 2-O-α-D-mannopyranosyl-α-D-mannopyranoside, a ligand for concanavalin A, from uniformly 13C-labelled D-glucose.

KW - C-enrichment

KW - Concanavalin A

KW - Man-α-1,2-Man-α-OMe

KW - NMR spectroscopy

UR - https://www.scopus.com/pages/publications/0031765221

M3 - Article

AN - SCOPUS:0031765221

SN - 1073-5070

VL - 3

SP - 217

EP - 222

JO - Carbohydrate Letters

JF - Carbohydrate Letters

IS - 3

ER -

Synthesis of 13C-labelled methyl α - D -mannopyranosyl-(1→2)-α-D-mannopyranoside from [U-13C]-D-glucose

Abstract

Keywords

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Cite this

Synthesis of ¹³C-labelled methyl α - D -mannopyranosyl-(1→2)-α-D-mannopyranoside from [U-¹³C]-D-glucose